A quick video to show you a voiceless demo on how to process 1D spectra with Mnova 11 in a simple manner. We have prepared a […]
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To shorten acquisition times and reduce file sizes most 2D spectra are typically acquired with far lower digital resolution than you would use for a 1D spectrum
Three tetranortriterpenoids were isolated as hemiacetals (the C-23 epimeric xylorumphiins M− O (4−6 )), which could not be purified due to the equilibration of the hemiacetal epimers in solution, hence giving complex spectra. In order to enable purification, compounds were acetylated and the R and S epimers could be separated. However, for these C-23 epimers, use of standard NOESY and ROESY techniques did not permit their differentiation, due to long distances between H-23 and protons from the main skeleton.
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